AVS 61st International Symposium & Exhibition
    Materials Characterization in the Semiconductor Industry Focus Topic Monday Sessions
       Session MC+2D+AP+AS-MoA

Paper MC+2D+AP+AS-MoA4
Electron Channeling Contrast Imaging: Examining Dislocation Effects in III-Ns

Monday, November 10, 2014, 3:00 pm, Room 313

Session: Characterization of III-Vs (2:00-3:20 pm)/Photovoltaics, EUV masks, etc. (3:40-4:40 pm)
Presenter: Michael Mastro, U.S. Naval Research Laboratory
Authors: J.K. Hite, U.S. Naval Research Laboratory
P. Gaddipati, American Society for Engineering Education
M.A. Mastro, U.S. Naval Research Laboratory
C.R. Eddy, U.S. Naval Research Laboratory
D.J. Meyer, U.S. Naval Research Laboratory
Correspondent: Click to Email

III-N materials continue to play a significant role in a range of technologies from rf electronics to visible and UV emitters and detectors. This is true despite a heavy population of extended defects in the active regions of these devices, which degrade the operation, potential performance, and reliability of such devices. With such high dislocation densities when grown heteroepitaxially on sapphire or SiC (108-1010 cm-2), techniques to reliably, rapidly, and non-destructively determine spatially defect density are necessary to determine the effects of these defects on device performance.

The most precise characterization tool for defect density has been transmission electron microscopy, but this is a destructive technique, as are other methods such as molten KOH or photo-electrochemical etching of the surface to reveal dislocation sites. Cathodoluminescence imaging only detects dislocations which change the optical emission of the material. X-ray diffraction can be used to extrapolate dislocation density, but not identify individual defects.

Electron channeling contrast imaging (ECCI), a non-destructive technique that has been used to examine defects in metals and ceramics, has recently seen use in III-nitride semiconductors. This technique allows for direct imaging of dislocations, grain boundaries, and topological information all at once. We will present an overview of the uses of ECCI in characterizing III-N materials, culminating in recent work applying the technique to AlGaN/GaN HEMT structures. By imaging the active areas of van der Pauw structures on a single sample with varying mobility, we find a direct negative correlation between screw dislocation and electron mobility.