AVS 65th International Symposium & Exhibition | |
Applied Surface Science Division | Thursday Sessions |
Session AS-ThP |
Session: | Applied Surface Science Division Poster Session |
Presenter: | Md. Nizam Sayeed, Old Dominion University |
Authors: | M.N. Sayeed, Old Dominion University U. Pudasaini, College of William and Mary H. E. Elsayed-Ali, Old Dominion University G. Eremeev, Thomas Jefferson National Accelerator Facility |
Correspondent: | Click to Email |
Nb3Sn is an intermetallic compound of A15 crystal structure that has type II superconductivity. Due to higher critical temperature Tc = 18.1 K and upper critical magnetic field of up to 30 T, Nb3Sn is considered as an alternative of niobium for Superconducting Radio Frequency (SRF) applications in particle accelerators. Nb3Sn coating on the inner surface of niobium SRF cavities can be operated at 4.2 K, whereas standard niobium cavities are currently operated at 2 K and consequently reduce the operation cost. However, synthesis of Nb3Sn is challenging due to the availability of other phases of niobium and tin (Nb6Sn5 and NbSn2), which have poor superconducting properties. We have fabricated Nb3Sn films on sapphire using multilayer sequential sputtering. Several thin layers of Nb and Sn were deposited repeatedly by magnetron sputtering and annealed afterward at 950 °C for 3 hours to form Nb3Sn. We have varied the Nb and Sn layer thicknesses of the films and characterized their crystal structure by X-ray diffraction (XRD), surface morphology by scanning electron microscopy (SEM), surface topography by atomic force microscopy (AFM), film stoichiometry by energy dispersive X-ray spectroscopy (EDS). The films showed crystalline structures of Nb3Sn only. Tc up to 17.63 K with sharp superconducting transition has been achieved.