AVS 65th International Symposium & Exhibition | |
Novel Trends in Synchrotron and FEL-Based Analysis Focus Topic | Thursday Sessions |
Session SA+AS+HC+SS-ThA |
Session: | IoT Session: Multi-modal Characterization of Energy Materials & Device Processing |
Presenter: | Trevor Willey, Lawrence Livermore National Laboratory |
Authors: | M.H. Nielsen, Lawrence Livermore National Laboratory J.A. Hammons, Lawrence Livermore National Laboratory M. Bagge-Hansen, Lawrence Livermore National Laboratory L.M. Lauderbach, Lawrence Livermore National Laboratory R. Hodgin, Lawrence Livermore National Laboratory K. Champley, Lawrence Livermore National Laboratory W. Shaw, Lawrence Livermore National Laboratory N. Sinclair, Washington State University T.M. Willey, Lawrence Livermore National Laboratory |
Correspondent: | Click to Email |
Radiographic imaging using a series of single pulses from synchrotron storage rings or x-ray free-electron lasers gives new insight into dynamic phenomena. One limitation of these sources is that the native and natural beam size at most end-station hutches is, at best, of mm-scale dimensions. Here, we describe a method for collecting full-field, radiographic images of cm-scale phenomena using focused pink-beam and scattering the x-rays, effectively creating point-source images. Although currently photon starved and highly dependent on parameters chosen (such as source-to-object and source-to-detector distances, scattering material, etc.) we are continuously improving the technique. At the Dynamic Compression Sector at the Advanced Photon Source, we use this capability to image detonation phenomena, particularly direct imaging of detonator performance, imaging initiation and run-up to detonation, imaging differences in ideal vs. non-ideal explosives, and have a goal to determining density during detonation at 10’s of microns in resolution. In this presentation, we summarize our progress developing and using this technique in creating movies of dynamic phenomena as fast as 153.4 ns between frames, and as a method for imaging samples prior to, for example, collecting dynamic small-angle x-ray scattering or diffraction to observe nanodiamond growth kinetics and composition evolution during detonation.