AVS 65th International Symposium & Exhibition | |
Processing and Characterization of Air-Liquid, Solid-Liquid and Air-Solid Interfaces Focus Topic | Tuesday Sessions |
Session PC+AS+BI+EM+NS+PB+SS-TuP |
Session: | Processing and Characterization of Gas-Liquid, Solid-Liquid, and Gas-Solid Interfaces |
Presenter: | Sonal Singhal, IIT Delhi, India |
Authors: | Sl. Singhal, IIT Delhi, India A.K. Shukla, IIT Delhi, India |
Correspondent: | Click to Email |
Superhydrophobic and superhydrophilic surfaces have been widely investigated due to their diverse range of applications such as self-cleaning, microfluidic application in biotechnology, corrosion, Anti-reflecting coatings and microelectronic mechanical system etc. Here, a facile chemical vapour deposition method is reported for the synthesis of carbon nanospheres (CNSs). Henceforth, the morphology of as-synthesized sample is characterized using scanning electron microscopy (SEM) and transmission electron microscopy (TEM). X-ray diffraction (XRD), Raman spectroscopy and FTIR spectroscopy are used to determine the phase purity, chemical composition and presence of chemical bonds on the surface of synthesized CNSs. TEM and SEM results reveal the presence of CNSs with a diameter ranging from 50 nm to 400 nm. Raman spectroscopy confirms the presence of disordered carbon and low graphitization, which are also confirmed by TEM and XRD results. Optical properties of as-synthesized CNSs is investigated by UV-Vis spectroscopy and photoluminescence. Wettability behaviour of as-synthesized carbon nanospheres is investigated by contact angle measurements. CNSs shows a water contact angle of 1520, which confirms the fabrication of superhydrophobic carbon nanosphere surface. After the proper explanation of wettability behaviour, it also discusses the application of as-synthesized CNSs as a photocatalyst. As it is well known, catalyst enhances the chemical reaction rate without changing its properties. Therefore, various kind of catalysts has been developed for the purpose to enhance the catalysis for environmental applications. Among different materials, carbon-based materials are widely used as a catalyst support due to their excellent properties. Considering these facts, the degradation of an organic pollutant under UV light is discussed here using CNSs.