AVS 59th Annual International Symposium and Exhibition
    Vacuum Technology Tuesday Sessions
       Session VT-TuP

Paper VT-TuP16
An Evaluation of the Outgassing Rates of Stainless Steel Vacuum Chambers Subjected to Different Heat Treatments and Coatings

Tuesday, October 30, 2012, 6:00 pm, Room Central Hall

Session: Vacuum Technology Poster Session and Student-built Vacuum System Poster Competition
Presenter: M.A. Mamun, Old Dominion University
Authors: M.A. Mamun, Old Dominion University
P.A. Adderley, Thomas Jefferson National Accelerator Facility
M.L. Stutzman, Thomas Jefferson National Accelerator Facility
M. Poelker, Thomas Jefferson National Accelerator Facility
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We present the results of an extensive study of the outgassing rates of four nominally identical stainless steel vacuum chambers. Chambers were either heat treated (semi-vacuum) at 400°C, coated with TiN, coated with SiO2 (SilcoGuard™), or heat treated then coated with SiO2. The outgassing rates were measured at a variety of room temperatures to determine the temperature dependence and compare to theoretical models of diffusion- or recombination-limited outgassing. In addition, outgassing rates were evaluated following venting to air and re-baking at 150°C and 250°C to simulate the impact of putting a chamber into service.