Paper SS-TuP7
A Novel Spectrometer for Wide Angle and High Pressure Photoemission
Tuesday, November 10, 2009, 6:00 pm, Room Hall 3
Session: |
Surface Science Poster Session I and Mort Traum Finalists |
Presenter: |
A. Thissen, SPECS GmbH, Germany |
Authors: |
A. Thissen, SPECS GmbH, Germany S. Mähl, SPECS GmbH, Germany T. Kampen, SPECS GmbH, Germany O. Schaff, SPECS GmbH, Germany |
Correspondent: |
Click to Email |
New scientific opportunities in key research fields like catalysis, research on liquid and aqueous samples, and living matter demand a combination of in-situ x-ray photoemission experiments (XPS) with high-pressure environments of up to 10 mbar.
To address these exciting new challenges we have developed a novel photoemission spectrometer that enables angle resolved photoelectron spectroscopy (XPS) at pressures up to 10 mbar with an angular acceptance of +/- 22°. This new set-up not only dramatically increases the spectrometer transmission but also allows non-destructive depth profiling exploiting the angular dependence of the XPS signal.
The instrument consists of a differentially pumped PHOIBOS 150 hemispherical analyzer with a pre-lens. This newly developed pre-lens increases the acceptance angle of the PHOIBOS analyzer by a factor of 5. At the same time it allows extremely efficient differential pumping of the gas atmosphere above the sample.