Pacific Rim Symposium on Surfaces, Coatings and Interfaces (PacSurf 2016)
    Nanomaterials Wednesday Sessions
       Session NM-WeP

Paper NM-WeP10
New Method Of Synthesis Of Graphene From Cvd In Steady State

Wednesday, December 14, 2016, 4:00 pm, Room Mauka

Session: Nanomaterials Poster Session
Presenter: Alejandra Moreno-Barcenas, Centro de Investigacion y de Estudios Avanzados Del Intituto Politecnico Nacional, Mexico
Authors: A. Moreno-Barcenas, Centro de Investigacion y de Estudios Avanzados Del Intituto Politecnico Nacional, Mexico
J.F. Perez-Robles, Centro de Investigacion y De Estudios Avanzados Del Intituto Politecnico Nacional, Mexico
A. Garcia-Garcia, Centro de Investigacion y De Estudios Avanzados Del Intituto Politecnico Nacional, Mexico
L.M. Avilez-Arellano, CINVESTAV Querétaro México, Mexico
Y.V. Vorobiev, CINVESTAV-Unidad Queretaro, Mexico
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The Graphene is a material used in a wide range of applications due to its unique structure and excellent electronic, optical, mechanical and thermal properties. Currently, several techniques are being developed to obtain graphene, one of this techniques that has highlighted which chemical vapor deposition (CVD) technique is the most reported. The fastest progress in graphene methodology in recent years have been obtained by this way. In this sense, the aim of the investigation in graphene is to increase the graphene production by CVD with high quality and at low cost. However, usually to produce graphene, it is necessary to use high vacuum equipment and temperatures about 1800 °C, which represents a very high cost. In this paper a new method is proposed to obtaining monolayer graphene with good quality and low cost operation. Using acetylene and nitrogen as precursors by CVD is possible to obtained monolayer graphene by CVD, instead of methane and argon. Also a mix of nitrogen:hydrogen (90:10, respectively) was used instead pure hydrogen. All the components are subjected to temperatures about 1000 °C and atmospheric pressure, on polycrystalline copper foil. The synthesis of the graphene is carried out in steady state, reducing the synthesis time around a minute. The amount of gas flow is determined taking into account the reactor volume per unit mass. The presence of graphene is shown by transmission electronic microscopy and Raman spectroscopy confirmed the monolayer of graphene.