AVS 60th International Symposium and Exhibition | |
Helium Ion Microscopy Focus Topic | Thursday Sessions |
Session HI-ThM |
Session: | Basics of Helium Ion Microscopy |
Presenter: | J.A. Notte, Carl Zeiss Microscopy |
Correspondent: | Click to Email |
The helium ion microscope (HIM) is now accepted as a valuable instrument on par with the SEM, the TEM, and Gallium FIB within the family of charged particle microscopes. The introduction of the HIM was sparked by the successful commercialization of the gas field ion source (GFIS), and several scientific papers have already addressed its principles of operation. However, at the opposite end of this instrument, secondary electron (SE) detector has received relatively little attention despite several interesting characteristics. This presentation will give an overview of the HIM’s SE detector and the unique circumstances in which it is used.
The SE detector on the HIM commonly operates under conditions and regimes that are distinctly different from the SEM. First, the overall efficiency is of prime importance since the excessive beam currents or excessive averaging often induce undesired sputtering or implantation in some samples. Generally, the areal dosages (measured ions / cm^2) that are required must be kept to a minimum, sufficient to achieve the minimum required signal to noise ratio (SNR) and the necessary field of view (FOV). Second, the probe current that is used in the HIM is commonly as small as 0.5 pA or less. While such small currents are adequate for high magnification imaging, the ions arrive infrequently with long intervals wherein no meaningful information is acquired. In contrast, for most charged particle microscopes the incident particles arrive so frequently that their resulting signals overlap. Third, when the incident ions do arrive, each one produces an abundance of secondary electrons - usually three or more – and substantially more for glancing angles. Thus, the amplitude of the detected signal conveys more information than the frequency of the pulses.
While some of these three conditions present challenges for the instrument and for the operator, they also represent a new regime for signal acquisition. Towards that end, a variety of new techniques have been tested with computer simulations and with real experiments. For example, pulse counting has been implemented with somewhat surprising results. Signal integration (as opposed to simple averaging) has also been thoroughly investigated on the instrument with very favorable results. Finally, a new imaging technique called ‘quotient mode’ has been investigated and seems to offer a unique advantage of a significantly improved SNR available to the HIM.